Ysi TruLab 1320P Manuel d'utilisateur

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OPERATIONS MANUAL
ba76157e01 03/2014
TruLab pH/ISE 1320(P)
PH/ISE METER
pH/ISE 1320P
pH/ISE 1320
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Résumé du contenu

Page 1 - TruLab pH/ISE 1320(P)

OPERATIONS MANUALba76157e01 03/2014TruLab pH/ISE 1320(P)PH/ISE METERpH/ISE 1320PpH/ISE 1320PrintermodulpH/ISE 1320PpH/ISE 1320

Page 2 - © 2014 Xylem Inc

Safety TruLab pH/ISE 1320 10 ba76157e01 03/20142.2 Safe operation2.2.1 Authorized useThis meter is authorized exclusively for pH, ORP and ISE concentr

Page 3 - TruLab pH/ISE 1320 - Contents

Glossary TruLab pH/ISE 1320 100 ba76157e01 03/2014Measured value The measured value is the special value of a measured parameter to be determined. It

Page 4 - 4 ba76157e01 03/2014

TruLab pH/ISE 1320 Indexba76157e01 03/2014 10117 IndexAAutomatic switch-off . . . . . . . . . . . . . . . . . . 20AutoReadORP . . . . . . . . . . . .

Page 5

Index TruLab pH/ISE 1320 102 ba76157e01 03/2014TTemperature measurementISE . . . . . . . . . . . . . . . . . . . . . . . . . . . .47pH . . . . . . .

Page 6 - Contents TruLab pH/ISE 1320

TruLab pH/ISE 1320 Contact Information103ba76157e01 03/201418 Contact Information18.1 Ordering & Technical SupportWhen placing an order please hav

Page 7 - 1 Overview

Contact Information TruLab pH/ISE 1320104ba76157e01 03/2014

Page 9 - 2 Safety

1) The tissue in plants that brings water upward from the roots;2) a leading global water technology company.We're 12,500 people unified in a com

Page 10 - 2.2 Safe operation

TruLab pH/ISE 1320 Commissioningba76157e01 03/2014 113 Commissioning3.1 Scope of delivery pH meter TruLab pH/ISE 1320  4 batteries 1.5 V Mignon type

Page 11 - 3 Commissioning

Commissioning TruLab pH/ISE 1320 12 ba76157e01 03/20143.3.1 Inserting the batteriesYou can operate the meter either with normal batteries or with rech

Page 12 - ± signs in

TruLab pH/ISE 1320 Commissioningba76157e01 03/2014 133.3.2 Connecting the power pack3.3.3 Mounting the standThe stand base can be mounted at the right

Page 13 - ECHNICAL DATA

Printer (only TruLab pH/ISE 1320 P) TruLab pH/ISE 1320 14 ba76157e01 03/20144 Printer (only TruLab pH/ISE 1320 P)4.1 Commissioning / switching the pri

Page 14 - 14 ba76157e01 03/2014

TruLab pH/ISE 1320 Printer (only TruLab pH/ISE 1320 P)ba76157e01 03/2014 154.2 Operation / printingData are only output to the printer if the followin

Page 15 - 4.4 Maintenance

Printer (only TruLab pH/ISE 1320 P) TruLab pH/ISE 1320 16 ba76157e01 03/20144.5 What to do if... / printer Integrated printer does not print Printer o

Page 16 - 16 ba76157e01 03/2014

TruLab pH/ISE 1320 Operationba76157e01 03/2014 175Operation5.1 General operating principles5.1.1 KeypadIn this operating manual, keys are indicated by

Page 17 - 5Operation

Operation TruLab pH/ISE 1320 18 ba76157e01 03/20145.1.2 Display5.1.3 Status information (meter)1 Status information (sensor)2 Measured value (with uni

Page 18 - 18 ba76157e01 03/2014

TruLab pH/ISE 1320 Operationba76157e01 03/2014 195.1.4 Socket field5.2 Switching on the meter1 pH electrode or ion selective electrode 12 Reference el

Page 19 - 5.2 Switching on the meter

2 ba76157e01 03/2014TruLab pH/ISE 1320For the most recent version of the manual, please visit www.ysi.com.Contact YSI 1725 Brannum Lane Yellow Springs

Page 20 - 5.4 Navigation

Operation TruLab pH/ISE 1320 20 ba76157e01 03/20145.3 Switching offAutomatic switch-off The instrument has an automatic switch-off function in order t

Page 21

TruLab pH/ISE 1320 Operationba76157e01 03/2014 21Only those displays and functions are available in the active operating mode that are currently being

Page 22

Operation TruLab pH/ISE 1320 22 ba76157e01 03/2014 Settings Settings are indicated by a colon. The current setting is displayed on the right-hand sid

Page 23

TruLab pH/ISE 1320 Operationba76157e01 03/2014 235.4.5 Example 1 on navigation: Setting the language1. Press the <On/Off> key. The measured valu

Page 24

Operation TruLab pH/ISE 1320 24 ba76157e01 03/20145. Select the General submenu with <><>. The current selection is displayed with a fr

Page 25 - 12.12.2012

TruLab pH/ISE 1320 Operationba76157e01 03/2014 255.4.6 Example 2 on navigation: Setting the date and timeThe measuring instrument has a clock with a d

Page 26 - 26 ba76157e01 03/2014

Operation TruLab pH/ISE 1320 26 ba76157e01 03/20147. If necessary, set the Date and Date format. The setting is made similarly to that of the time.8.

Page 27 - 5.5 Channel display

TruLab pH/ISE 1320 Operationba76157e01 03/2014 275.5 Channel displayThe TruLab pH/ISE 1320 manages the connected sensors and displays which sensor is

Page 28 - 6 pH value

pH value TruLab pH/ISE 1320 28 ba76157e01 03/20146 pH value6.1 Measuring6.1.1 Measuring the pH valueNOTE When connecting an earthed PC/printer, measur

Page 29 - ∆ : better than 0.5 °C

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 29Criteria for a stable measured valueThe Stability control function checks whether the measured values

Page 30 - Temp. measurement

TruLab pH/ISE 1320 - ContentsTruLab pH/ISE 1320 Contentsba76157e01 03/2014 31 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

Page 31 - 6.2 Calibration

pH value TruLab pH/ISE 1320 30 ba76157e01 03/20146.1.2 Measuring the temperatureFor reproducible pH measurements, it is essential to measure the tempe

Page 32 - 32 ba76157e01 03/2014

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 316.2 Calibration6.2.1 Why calibrate?pH electrodes age. This changes the zero point (asymmetry) and slop

Page 33

pH value TruLab pH/ISE 1320 32 ba76157e01 03/2014Continuing with two-point calibration5. Thoroughly rinse the electrode with deionized water.6. Immers

Page 34 - 34 ba76157e01 03/2014

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 33Continuing with three- to five-point calibration14. Start the measurement with <ENTER>.The measu

Page 35 - 7.000

pH value TruLab pH/ISE 1320 34 ba76157e01 03/20146.2.4 Manual calibration (ConCal)Make sure that in the sensor menu, Buffer menu, the ConCal buffer se

Page 36 - 4.035

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 35Continuing with two-point calibration7. When measuring without temperature sensor:Enter the temperatur

Page 37 - 9.958

pH value TruLab pH/ISE 1320 36 ba76157e01 03/2014Continuing with three- to five-point calibration14. Immerse the electrode in the second buffer soluti

Page 38 - 38 ba76157e01 03/2014

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 376.2.5 Calibration pointsCalibration can be performed using one to five buffer solutions in any order (

Page 39 - DO IF..., page 89)

pH value TruLab pH/ISE 1320 38 ba76157e01 03/20146.2.6 Calibration dataDisplaying the calibration data The calibration record of the last calibration

Page 40 - 40 ba76157e01 03/2014

TruLab pH/ISE 1320 pH valueba76157e01 03/2014 39Calibration record (example)Display Calibration recordZero point [mV]Slope [mV/pH]+++- 15 ... + 15 -6

Page 41 - 157.0 mV

Contents TruLab pH/ISE 1320 4 ba76157e01 03/20145.4.4 Elements in menus and dialogs . . . . . . . . . . . . . . . . . . . 215.4.5 Example 1 on navig

Page 42 - ∆ : better than 0.3 mV

pH value TruLab pH/ISE 1320 40 ba76157e01 03/20146.2.7 Continuous measurement control (CMC function) The Continuous Measurement Control (CMC funct

Page 43 - USB output

TruLab pH/ISE 1320 ORP voltageba76157e01 03/2014 417 ORP voltage7.1 Measuring7.1.1 Measuring the ORPNOTE When connecting an earthed PC/printer, measur

Page 44 - 7.2 ORP calibration

ORP voltage TruLab pH/ISE 1320 42 ba76157e01 03/2014The minimum duration until a measured value is assessed as stable is the monitored time interval.

Page 45 - 0.157 mg/l

TruLab pH/ISE 1320 ORP voltageba76157e01 03/2014 437.1.2 Measuring the relative ORPTo measure the difference of the ORPs of two solutions, you have to

Page 46 - 46 ba76157e01 03/2014

ORP voltage TruLab pH/ISE 1320 44 ba76157e01 03/2014The minimum duration until a measured value is assessed as stable is the monitored time interval.

Page 47

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 458 Ion concentration8.1 Measuring8.1.1 Measuring the ion concentration NOTE When connecting an

Page 48 - 0.010 mg/l

Ion concentration TruLab pH/ISE 1320 46 ba76157e01 03/2014 as soon as the measured value is outside the stability range  when the automatic Stabilit

Page 49 - 0.020 mg/l

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 478.1.2 Measuring the temperatureFor reproducible ion-selective measurements, it is essential t

Page 50 - 8.9

Ion concentration TruLab pH/ISE 1320 48 ba76157e01 03/20148.2 Calibration8.2.1 Why calibrate?Ion-selective electrodes age and are temperature-dependen

Page 51

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 49Continuing with two-point calibration7. Thoroughly rinse the electrode with distilled water.8

Page 52

TruLab pH/ISE 1320 Contentsba76157e01 03/2014 59.3 Sensor-independent settings . . . . . . . . . . . . . . . . . . . . . . . . . . 759.3.1 System .

Page 53

Ion concentration TruLab pH/ISE 1320 50 ba76157e01 03/2014 Continuing with three- to seven-point calibrationRepeat the steps 8 to 13 in the same way w

Page 54 - ING METHOD, page 53)

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 518.2.4 Calibration standardsUse two to seven different standard solutions. The standard soluti

Page 55

Ion concentration TruLab pH/ISE 1320 52 ba76157e01 03/2014Calibration evaluationAfter calibrating, the meter automatically evaluates the calibration.C

Page 56

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 538.3 Selecting the measuring methodThe following methods are supported: Standard addition St

Page 57

Ion concentration TruLab pH/ISE 1320 54 ba76157e01 03/20148.3.1 Standard additionIn the "Standard addition" procedure, a known amount of sta

Page 58 - 58 ba76157e01 03/2014

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 5511. Select Continue with <> <> and start the measurement with <MENU/ENTER>

Page 59

Ion concentration TruLab pH/ISE 1320 56 ba76157e01 03/20148.3.2 Standard subtractionIn the "Standard Subtraction" procedure, a known amount

Page 60 - Sample addition

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 5710. Using <> <> and <MENU/ENTER>, select the values for the vol-ume of th

Page 61

Ion concentration TruLab pH/ISE 1320 58 ba76157e01 03/201419. Confirm Yes with <MENU/ENTER>. Measurement with the selected method is completed.

Page 62

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 598.3.3 Sample additionIn the "Sample addition" procedure, a known amount of sample i

Page 63

Contents TruLab pH/ISE 1320 6 ba76157e01 03/2014

Page 64

Ion concentration TruLab pH/ISE 1320 60 ba76157e01 03/201411. Select Continue with <> <> and start the measurement with <MENU/ENTER&g

Page 65

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 618.3.4 Sample subtractionWith the "Sample subtraction" procedure, a known amount of

Page 66 - 9 Settings

Ion concentration TruLab pH/ISE 1320 62 ba76157e01 03/2014Measuring7. Start the measurement with <F1> Continue. An entry window appears.8. Prepa

Page 67 - TION, page 31)

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 638.3.5 Standard addition with blank value correction (Blank value addition) In the "S

Page 68 - 68 ba76157e01 03/2014

Ion concentration TruLab pH/ISE 1320 64 ba76157e01 03/2014MeasuringCALIBRATION12.12.2012 12:12:12#1 0.010 mg/l 20.2 mV 25.0 °C#2 0.100 mg/l 79.2 mV

Page 69

TruLab pH/ISE 1320 Ion concentrationba76157e01 03/2014 6512. Add the standard solution to the sample.13. Using <> <> and <MENU/ENTER&

Page 70 - 70 ba76157e01 03/2014

Settings TruLab pH/ISE 1320 66 ba76157e01 03/20149 Settings9.1 Measurement settings9.1.1 Settings for pH measurementsThe settings for pH measurements

Page 71 - * 4.000

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 67Calibration/ Serial number (sen-sor)- Entry of the series number of the connected sensor. The series n

Page 72 - 72 ba76157e01 03/2014

Settings TruLab pH/ISE 1320 68 ba76157e01 03/20149.1.2 Buffer sets for calibrationYou can use the buffer sets quoted in the table for an automatic cal

Page 73

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 69No. Buffer set * pH values at1 YSI * 4.0007.00010.00025 °C2 ConCal Any Any3 NIST/DINDIN buffers accord

Page 74 - 74 ba76157e01 03/2014

TruLab pH/ISE 1320 Overviewba76157e01 03/2014 71 Overview1.1 TruLab pH/ISE 1320 meterThe compact precision pH meter TruLab pH/ISE 1320 enables you to

Page 75

Settings TruLab pH/ISE 1320 70 ba76157e01 03/201413 Fisher * 2.0074.0027.00410.00225 °C14 Fluka BS * 4.0066.9848.95725 °C15 Radiometer * 1.6784.0057

Page 76 - 9.4 Reset

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 71* Brand names or trade names are trademarks of their respective owners protected by law.9.1.3 Calibrat

Page 77

Settings TruLab pH/ISE 1320 72 ba76157e01 03/20149.1.4 Settings for ORP measurementsThe settings for ORP measurements are made in the menu for calibra

Page 78 - 10 Data storage

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 739.2 Settings for ISE measurementsThe settings are made in the measuring menu of the ISE measurement. T

Page 79 - MENT DATA STORAGE, page 83)

Settings TruLab pH/ISE 1320 74 ba76157e01 03/2014Man. temperature -25 ... +25 ... +130 °C Entry of the manually deter-mined temperature. For measureme

Page 80 - 0d03h00min

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 759.3 Sensor-independent settings9.3.1 SystemTo open the Storage & config menu, press the <MENU/E

Page 81 - 10.3 Measurement data storage

Settings TruLab pH/ISE 1320 76 ba76157e01 03/20149.3.2 Data storageThis menu contains all functions to display, edit and erase stored measured values

Page 82

TruLab pH/ISE 1320 Settingsba76157e01 03/2014 77The sensor settings are reset under the Reset menu item in the menu for cali-bration and measurement s

Page 83 - DITING THE

Data storage TruLab pH/ISE 1320 78 ba76157e01 03/201410 Data storageYou can transmit measured values (datasets) to the data storage: Manual data stor

Page 84

TruLab pH/ISE 1320 Data storageba76157e01 03/2014 79You have the following options: To erase the entire storage, confirm Yes. To cancel the storage

Page 85 - 11.3 MultiLab Importer

Overview TruLab pH/ISE 1320 8 ba76157e01 03/20141.2 TruLab pH/ISE 1320P meterThe integrated printer of the TruLab pH/ISE 1320 P enables to document me

Page 86 - 86 ba76157e01 03/2014

Data storage TruLab pH/ISE 1320 80 ba76157e01 03/2014Settings You can configure the automatic data storage function with the following settings:Starti

Page 87 - 12.1 Maintenance

TruLab pH/ISE 1320 Data storageba76157e01 03/2014 81Energy saving mode ([Eco mode])If the automatic storing function is active, the meter provides an

Page 88 - 12.4 Disposal

Data storage TruLab pH/ISE 1320 82 ba76157e01 03/2014SettingsDisplay presentation of a datasetRepresentation of a dataset (USB output)Menu item Settin

Page 89 - 13 What to do if

TruLab pH/ISE 1320 Data storageba76157e01 03/2014 83Quitting the display To quit the display of stored measurement datasets, you have the following op

Page 90 - 90 ba76157e01 03/2014

TruLab pH/ISE 1320 Transmitting data (USB interface)ba76157e01 03/2014 8411 Transmitting data (USB interface) 11.1 Options for data transmissionVia th

Page 91 - 13.2 ISE

TruLab pH/ISE 1320 Transmitting data (USB interface)ba76157e01 03/2014 8511.2 Connecting a PC Connect the TruLab pH/ISE 1320 to the PC via the USB in

Page 92 - 92 ba76157e01 03/2014

Transmitting data (USB interface) TruLab pH/ISE 1320 86 ba76157e01 03/2014

Page 93 - 13.3 General information

TruLab pH/ISE 1320 Maintenance, cleaning, disposalba76157e01 03/2014 8712 Maintenance, cleaning, disposal12.1 Maintenance12.1.1 General maintenance ac

Page 94 - 14 Technical data

Maintenance, cleaning, disposal TruLab pH/ISE 1320 88 ba76157e01 03/201412.2 CleaningOccasionally wipe the outside of the measuring instrument with a

Page 95

TruLab pH/ISE 1320 What to do if...ba76157e01 03/2014 8913 What to do if...13.1 pH/ORPError message OFL, UFLThe measured value is outside the measurin

Page 96 - 14.2 General data

TruLab pH/ISE 1320 Safetyba76157e01 03/2014 92 Safety2.1 Safety information2.1.1 Safety information in the operating manualThis operating manual provi

Page 97

What to do if... TruLab pH/ISE 1320 90 ba76157e01 03/2014No stable measured value Obviously incorrect measured valuesCause RemedypH electrode:– Juncti

Page 98 - 15 Firmware update

TruLab pH/ISE 1320 What to do if...ba76157e01 03/2014 9113.2 ISEError message OFL Obviously incorrect measured valuesError message, Error (invalid cal

Page 99 - 16 Glossary

What to do if... TruLab pH/ISE 1320 92 ba76157e01 03/2014

Page 100 - 100 ba76157e01 03/2014

TruLab pH/ISE 1320 What to do if...ba76157e01 03/2014 9313.3 General informationSensor symbol flashes displayMeter does not react to keystrokeYou want

Page 101 - 17 Index

Technical data TruLab pH/ISE 1320 94 ba76157e01 03/201414 Technical data 14.1 Measuring ranges, resolution, accuracy14.1.1 pH/ORPMeasuring ranges, re

Page 102 - 102 ba76157e01 03/2014

TruLab pH/ISE 1320 Technical databa76157e01 03/2014 9514.1.2 ISEMeasuring ranges, resolutionParameter Measuring range ResolutionISE [mg/l] 0.000 ...

Page 103 - 18 Contact Information

Technical data TruLab pH/ISE 1320 96 ba76157e01 03/201414.2 General dataDimensions TruLab pH/ISE 1320: Approx. 230 x 190 x 80 mmTruLab pH/ISE 1320 P:A

Page 104

TruLab pH/ISE 1320 Technical databa76157e01 03/2014 97Applicable directives and standardsEMC EC directive 2004/108/ECEN 61326-1EN 61000-3-2EN 61000-3-

Page 105

Firmware update TruLab pH/ISE 1320 98 ba76157e01 03/201415 Firmware updateAvailable firmware updates are provided on the Internet. With the firmware u

Page 106 - Xylem

TruLab pH/ISE 1320 Glossaryba76157e01 03/2014 9916 GlossarypH/ORP/ISEGeneral informationAsymmetry see zero pointElectromotive force of a electrodeThe

Modèles reliés TruLab 1320

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